Lipase-ultrasound assisted synthesis of polyesters
نویسندگان
چکیده
منابع مشابه
Ultrasound Assisted Green Synthesis and Characterization of Graphene Oxide
Graphene oxide (GO) was prepared by an improved green chemical method using graphite flakes, KMnO4, a mixture of H2SO4/H3PO4, H2O2 and HCl. In several stages, ultrasound was used to separate the oxidized layers of GO. The use of ultrasound optimizes the effect of the reacting agents, decreasing the required amou...
متن کاملLipase-catalyzed syntheses of telechelic polyesters
Telechelic polyesters have successfully been synthesized with lipasecatalyzed polymerization. The produced telechelics had a high degree of difunctionalization, high purity (requiring little or no workup) and controlled degree of polymerization. The syntheses were performed in one-pot one-step reaction systems. Two different types of lipase-catalyzed polymerizations were applied – ring-opening ...
متن کاملUltrasound-assisted lipase-catalyzed synthesis of D-isoascorbyl palmitate: process optimization and Kinetic evaluation
BACKGROUND D-isoascorbic acid is a food antioxidant additive and used in accordance with Good Manufacturing Practice (GMP). High solubility in water (about 150 g/L at 25°C) reduces its effectiveness in stabilizing fats and oils. Our research group had successfully synthesized D-isoascorbyl palmitate using immobilized lipase Novozym 435 as a biocatalyst. Low production efficiency of D-isoascorby...
متن کاملUltrasound-assisted lipase catalyzed hydrolysis of aspirin methyl ester.
The ultrasound-assisted hydrolysis of aspirin methyl ester (AME) was investigated using immobilized Candida antarctica lipase B (CALB) (1%) in the presence of solvents like triolein, chloroform (CHCl3) and dichloromethane (DCM). The effect of ultrasound and the role of water on the conversion rates have also been investigated. Proton nuclear magnetic resonance spectroscopic (1H NMR) was chosen ...
متن کاملUltrasound assisted interfacial synthesis of gold nanocones.
This communication describes a facile method for the synthesis of conical-shaped Au nanoparticles with a hollow cavity by combining interfacial reaction and ultrasonic cavitation. The Au nanocones showed an enhancement factor of 7.7 × 10(8) in surface enhanced Raman scattering (SERS) detection.
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Ultrasonics Sonochemistry
سال: 2017
ISSN: 1350-4177
DOI: 10.1016/j.ultsonch.2017.03.051